SYNTHESIS AND PROPERTIES OF LITHIUM TETRAKIS(TRIMETHYLSILYL)ALUMINATE COMPLEXES

被引：19

作者：

ROSCH, L

ALTNAU, G

机构：

来源：

CHEMISCHE BERICHTE-RECUEIL | 1979年 / 112卷 / 12期

关键词：

D O I：

10.1002/cber.19791121217

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Synthesis and Properties of Lithium Tetrakis(trimethylsilyl)aluminate Complexes Chlorotrimethylsilane reacts with aluminium and lithium in ether in the presence of mercury to form lithium tetrakis(trimethylsilyl)aluminate, coordinated with diethyl ether, tetrahydrofurane, or dimethoxyethane. Unsolvated lithium tetrakis(trimethylsilyl)aluminate results by repeated sublimation of the ether adduct. The IR, Raman, and NMR spectra are discussed. Copyright © 1979 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim

引用

页码：3934 / 3938

页数：5

共 13 条

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[9] ROSCH L, UNPUBLISHED
[10] ROSCH L, 1977, ANGEW CHEM, V89, P497

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