APPLICATION OF MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY TO THE ANALYSIS OF PESTICIDES

被引:19
作者
SUSSE, H [1 ]
MULLER, H [1 ]
机构
[1] UNIV HALLE WITTENBERG,INST ANALYT & UMWELTCHEM,D-06217 MERSEBURG,GERMANY
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1995年 / 352卷 / 05期
关键词
D O I
10.1007/BF00323368
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A method for the simultaneous separation and determination of selected triazines, carbamates and phosphororganic compounds by micellar electrokinetic capillary electrophoresis has been developed. A mixture of nine pesticides has been investigated with respect to optimize their separation as a function of buffer and surfactant character and concentration, organic modifier and buffer pH. Quantitative aspects have been also examined. A determination of the compounds was possible up to the range of 0.1 mg/l. Best results have been achieved using a borate/SDS buffer, pH 8. At an applied voltage of 20 kV, the investigated compounds have been successfully resolved within 13 min.
引用
收藏
页码:470 / 473
页数:4
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