USE OF SILYLATING AGENTS FOR IDENTIFICATION OF HYDROXYLATED STEROIDS BY GAS-CHROMATOGRAPHY AND GAS CHROMATOGRAPHY MASS SPECTROMETRY - DISCRIMINATION BETWEEN PHENOLIC AND ALCOHOLIC HYDROXYL-GROUPS

被引：8

作者：

MIYAZAKI, H

ISHIBASHI, M

ITOH, M

YAMASHITA, K

NAMBARA, T

机构：

[1] NIPPON KAYAKU CO,DIV PHARMACEUT,RES LABS,KITA KU,TOKYO,JAPAN

[2] TOHOKU UNIV,INST PHARMACEUT,SENDAI,MIYAGI 980,JAPAN

来源：

JOURNAL OF CHROMATOGRAPHY | 1977年 / 133卷 / 02期

关键词：

D O I：

10.1016/S0021-9673(00)83488-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

引用

页码：311 / 318

页数：8

共 12 条

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[3] IMPROVED METHOD FOR SPECIFIC RELEASE OR ACYLATION OF PRIMARY HYDROXYL-GROUPS FROM PERTRIMETHYLSILYLATED POLYOLS
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[J]. CHEMISCHE BERICHTE-RECUEIL, 1974, 107 (02): : 721 - 724
[4] SOME STEREOCHEMICAL FACTORS IN FORMATION OF REARRANGEMENT IONS IN MASS SPECTRA OF TRIMETHYLSILYL DERIVATIVES OF STEROIDAL PHOSPHATES
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[5] MASS-SPECTRA OF TRIMETHYLSILYL DERIVATIVES OF GLYCEROPHOSPHORIC ACIDS - INTER-MOLECULAR AND INTRA-MOLECULAR REARRANGEMENTS OF SILICONIUM IONS
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[6] GAS-CHROMATOGRAPHIC SEPARATION OF PHYTOECDYSONES
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ISHIBASHI, M
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[7] LAWSON AM, 1971, J AM CHEM SOC, V93, P1014
[8] MASS-SPECTRA OF PROSTAGLANDINS .1. TRIMETHYLSILYL AND ALKYLOXIME-TRIMETHYLSILYL DERIVATIVES OF PROSTAGLANDIN-A1
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[J]. PROSTAGLANDINS, 1973, 4 (01): : 31 - 46
[9] MASS-SPECTROMETRY IN ANALYSIS OF STEROID DRUGS AND THEIR METABOLITES - ELECTRON-IMPACT-INDUCED FRAGMENTATION OF RING-D
MIDDLEDITCH, BS
VOUROS, P
BROOKS, CJW
[J]. JOURNAL OF PHARMACY AND PHARMACOLOGY, 1973, 25 (02) : 143 - 149
[10] MIYAZAKI H, 1975, CHEM PHARM BULL, V23, P3033

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