THIN-LAYER CHROMATOGRAPHY OF ECDYSTEROIDS ORIGINATED FROM SILENE-OTITES L (WIB)

被引:11
作者
BATHORI, M
SZENDREI, K
KALASZ, H
LAFONT, R
GIRAULT, JP
机构
[1] SEMMELWEIS UNIV MED, DEPT PHARMACOL, H-1085 BUDAPEST 8, HUNGARY
[2] ECOLE NORMALE SUPER, F-75231 PARIS 05, FRANCE
[3] UNIV PARIS 05, CHIM & BIOCHIM PHARMACOL & TOXICOL LAB, F-75270 PARIS 06, FRANCE
关键词
D O I
10.1007/BF02327660
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Thin-layer chromatographic investigations of ecdysteroids have been carried out to monitor their isolation by column chromatography and droplet countercurrent chromatography as well as to control the homogeneity of the pure products. Isolation scheme and chemical structure of the 20-hydroxyecdysone-22-benzoate and that of three new ecdysteroid compounds, 2-deoxy-1,20-dihydroxyecdysone, 2-deoxyecdysone-22-acetate and 2-deoxy-20-hydroxyecdysone-22-acetate are also presented.
引用
收藏
页码:627 / 630
页数:4
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