ULTRASMALL-ANGLE X-RAY-SCATTERING STUDIES OF HETEROGENEOUS SYSTEMS USING SYNCHROTRON RADIATION TECHNIQUES

被引:11
作者
NORTH, AN
DORE, JC
MACKIE, AR
HOWE, AM
HARRIES, J
机构
[1] INST FOOD RES, NORWICH NR4 7UA, NORFOLK, ENGLAND
[2] SERC, DARESBURY LAB, WARRINGTON WA4 4AD, CHESHIRE, ENGLAND
关键词
D O I
10.1016/0168-583X(90)90758-M
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Ultrasmall-angle X-ray scattering (USAXS) studies of heterogeneous systems are reported. The twin-crystal diffractometer developed by Bonse and Hart was used in combination with the high-intensity X-ray beams from a synchrotron radiation source. With this experimental configuration, scattering profiles were obtained over a Q-range of 5×10-5≤Q≤10-2Å-1 giving information on the length scale 15 nm to 1 μm. In the present paper USAXS studies of three systems are reported: a particulate system (latex), a system displaying aggregation properties (microemulsion) and a porous solid (oil-bearing shale). Experimental procedure and data analysis techniques are discussed. A short comparison is made of synchrotron radiation USAXS and other techniques. © 1990.
引用
收藏
页码:283 / 290
页数:8
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