ADDUCT OF 2 1,8-NAPHTHYRIDINE MOLECULES (ONE PROTONATED) WITH TETRACHLOROFERRATE(III)

被引：13

作者：

BARBARO, P

BIANCHINI, C

FOCHI, M

MASI, D

MEALLI, C

机构：

[1] Istituo per lo Studio della Stereochimica ed Energetica dei Composti di Coordinazione, CNR, Via J. Nardi 39, Firenze

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1992年 / 48卷

关键词：

D O I：

10.1107/S0108270191011149

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

1,8-Naphthyridinium tetrachloroferrate(III)-1,8-naphthyridine (1/1), C8H7N2+.FeCl4-.-C8H6N2, M(r) = 458.9, monoclinic, Cc, a = 10.698 (2), b = 25.533 (4), c = 7.315 (2) angstrom, beta = 101.83 (1)-degrees, V = 1955.67 (72) angstrom 3, Z = 4, D(x) = 1.5588 Mg m-3, lambda(Cu K-alpha) = 1.5418 angstrom, mu = 11.4 mm-1, F(000) = 924, room temperature, final R = 0.0704 for 929 reflections. The structure consists of discrete tetrahedral FeCl4- anions, protonated (NNH)+ and unprotonated (NN) 1,8-naphthyridine molecules.

引用

页码：625 / 627

页数：3

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