STRUCTURE AND REACTIVITY OF LITHIUM AMIDES - LI-6,C-13, AND N-15 NMR SPECTROSCOPIC STUDIES AND COLLIGATIVE MEASUREMENTS OF LITHIUM DIPHENYLAMIDE AND LITHIUM DIPHENYLAMIDE-LITHIUM BROMIDE COMPLEX SOLVATED BY TETRAHYDROFURAN

被引：86

作者：

DEPUE, JS ^{[1
]}

COLLUM, DB ^{[1
]}

机构：

[1] CORNELL UNIV,BAKER LAB,DEPT CHEM,ITHACA,NY 14853

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 1988年 / 110卷 / 16期

关键词：

D O I：

10.1021/ja00224a041

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

引用

页码：5518 / 5524

页数：7

共 92 条

[1] THE LADDERING PRINCIPLE IN LITHIUM AMIDE CHEMISTRY - THE CRYSTAL AND MOLECULAR-STRUCTURE OF THE PYRROLIDIDOLITHIUM ADDUCT [H2C(CH2)3NLI]3.MEN(CH2CH2NME2)2 [J].

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[2] THE RING-STACKING PRINCIPLE IN ORGANOLITHIUM CHEMISTRY - ITS DEVELOPMENT THROUGH THE ISOLATION AND CRYSTAL-STRUCTURES OF HEXAMERIC IMINOLITHIUM CLUSTERS (RR'C=NLI)6(R'=PH,R=BU-T OR ME2N,R=R'=ME2N OR BU-T) [J].

ARMSTRONG, DR ;

BARR, D ;

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JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1987, (05) :1071-1081

[3]

ARMSTRONG DR, IN PRESS J CHEM S DA

[4] METALATION OF AMINOSILANES - PREPARATION, INFRARED AND H-1 AND LI-7 NMR-SPECTRA OF MONO-LITHIATED AND POLY-LITHIATED DERIVATIVES OF (SI-N-BUTYLAMINO)METHYLSILANES (SILAZATES) [J].

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[5]

BARR B, 1984, J CHEM SOC CHEM COMM, P79

[6] 3 MODEL STRUCTURAL TYPES IN LITHIUM AMIDE CHEMISTRY - THE CRYSTAL AND MOLECULAR-STRUCTURES OF DIMERIC [PH(ME)NLI.ME2NCH2CH2NME2]2 AND MONOMERIC PH(NAPHTHYL)NLI.MEN(CH2CH2NME2)2 AND OF [PH(NAPHTHYL)NLI.TMEDA]2, A LOOSE DIMER [J].

BARR, D ;

CLEGG, W ;

MULVEY, RE ;

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JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1987, (10) :716-718

[7] THE SYNTHESES AND CRYSTAL-STRUCTURES OF 2 IMINOLITHIUM ADDUCTS - (PH2C=NLI.NC5H5)4, A TETRAMERIC PSEUDO-CUBANE FORMED BY STACKING 2 (LIN)2 4-MEMBERED RINGS, AND [BUT2C=NLI.OP(NME2)3]2, A DIMER PREVENTED STERICALLY FROM STACKING [J].

BARR, D ;

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JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1987, (09) :2141-2147

[8] ISOLATION AND SOLUTION STRUCTURES OF (PHCH2NLICH2CH2NME2)N AND OF THE TOTALLY RIGID DILITHIUM COMPOUND, (ORTHO-LIC6H4CH2NLICH2CH2NME2)N - EVIDENCE FOR LI ... ORTHO-HC INTERACTIONS [J].

BARR, D ;

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JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1987, 325 (1-2) :C1-C6

[9] THE STRUCTURAL ISOMERS OF ([PH(2-PYRIDYL)NLI].[O=P(NME2)3])2 - DIMERIC SPECIES WITH ALTERNATIVE CENTRAL (LIN)2 AND (LIO)2 RINGS, THE LATTER INVOLVING UNPRECEDENTED NEUTRAL BRIDGING OXYGEN LIGANDS [J].

BARR, D ;

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JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (11) :700-701

[10] THE ISOLATION AND CRYSTAL-STRUCTURE OF "[PH(2-PYR)NLI].(HMPA).[PH(2-PYR)NH] - A MODEL MONOMERIC ORGANONITROGEN LITHIUM SPECIES CONTAINING COORDINATION OF LITHIUM BY BOTH AN ANCHIMERIC PYRIDYL N-ATOM AND BY A POTENTIALLY REACTIVE AMINE LIGAND [J].

BARR, D ;

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JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (07) :469-470

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