DETERMINATION OF LEAD BY HYDRIDE GENERATION ATOMIC-ABSORPTION SPECTROMETRY .1. A NEW MEDIUM FOR GENERATING HYDRIDE

被引:32
作者
LI, JX [1 ]
LIU, YM [1 ]
LIN, TZ [1 ]
机构
[1] ACAD SINICA,DALIAN INST CHEM PHYS,161 ZHONGSHAN RD,DALIAN,PEOPLES R CHINA
关键词
D O I
10.1016/S0003-2670(00)86412-0
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A new medium, used to generate lead hydride, was optimized as 0.3% (w/v) oxalic acid-2% (w/v) ammonium cerium (III) nitrate-8% (w/v) potassium tetrahydroborate-1% (w/v) sodium hydroxide solution; 950°C is used for atomization. The characteristic concentration (0.0044 absorbance) obtained under these conditions was 0.04 ng ml-1. The application of this medium to soil and ferromagano-brass samples is illustrated. © 1990.
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页码:151 / 155
页数:5
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