STRUCTURE OF [1,2-BIS(DIPHENYLPHOSPHINO)ETHANE]DI(PHENYLTHIO)PALLADIUM(II)

被引：14

作者：

WEI, GW

LIU, HQ

机构：

[1] ACAD SINICA,FUJIAN INST RES STRUCT MATTER,FUZHOU 350002,PEOPLES R CHINA

[2] ACAD SINICA,FUZHOU LAB STRUCT CHEM,FUZHOU 350002,PEOPLES R CHINA

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1990年 / 46卷

关键词：

D O I：

10.1107/S0108270190006321

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

[Pd(C6H5S)2{(C6H5)2PCH2CH2P(C6H5)2}], M(r) = 723.17, monoclinic, C2/c, a = 14.320 (2), b = 16.383 (2), c = 14.295 (2) angstrom, beta = 93.41 (2)-degrees, V = 3347.7 (9) angstrom 3, Z = 4, D(x) = 1.435 g cm-3, Mo K-alpha radiation, lambda = 0.71073 angstrom, mu = 7.856 cm-1, F(000) = 1480, T = 296 (1) K, R = 0.0269 for 3084 reflections with I > 3-sigma(I). The molecule possesses a twofold axis passing through Pd and the midpoints of S-S and P-P with these five atoms being essentially coplanar.

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页码：2457 / 2458

页数：2

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