GAS-CHROMATOGRAPHIC MASS-SPECTROMETRIC METHOD FOR THE SIMULTANEOUS DETERMINATION OF AMITRAZ, BROMOPROPYLATE, COUMAPHOS, CYMIAZOLE AND FLUVALINATE RESIDUES IN HONEY

被引：35

作者：

MUINO, MAF ^{[1
]}

LOZANO, JS ^{[1
]}

机构：

[1] UNIV SANTIAGO DE COMPOSTELA,FAC FARM,AREA NUTR & BROMATOL,E-15706 SANTIAGO,SPAIN

来源：

ANALYST | 1993年 / 118卷 / 12期

关键词：

ACARICIDE RESIDUES; AMITRAZ; BROMOPROPYLATE; COUMAPHOS; CYMIAZOLE AND FLUVALINATE; HONEY; GAS CHROMATOGRAPHY; MASS SPECTROMETRY;

D O I：

10.1039/an9931801519

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A rapid method for determining acaricide residues in honey is proposed. After dissolving honey samples in water, acaricides are subjected to solid-phase extraction with a Sep-Pak C-18 cartridge and directly determined by gas chromatography-mass spectrometry. The quantification limit obtained for different acaricides ranged from 10 to 40 mu g kg(-1) and recoveries from spiked honey samples averaged 85% and ranged from 74 to 96%.

引用

页码：1519 / 1522

页数：4

共 19 条

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