SCREENING FOR AMINES BY DANSYLATION AND AUTOMATED HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：35

作者：

PRICE, NPJ

FIRMIN, JL

GRAY, DO

机构：

[1] UNIV LONDON,QUEEN MARY & WESTFIELD COLL,SCH BIOL SCI,LONDON E1 4NS,ENGLAND

[2] JOHN INNES INST,JOHN INNES CTR PLANT SCI RES,NORWICH NR4 7UH,NORFOLK,ENGLAND

来源：

JOURNAL OF CHROMATOGRAPHY | 1992年 / 598卷 / 01期

关键词：

D O I：

10.1016/0021-9673(92)85113-8

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A reversed-phase high-performance liquid chromatographic procedure for the determination of a broad range of amines after derivatization with dansyl chloride is presented. Forty-five amines were tested over the concentration range 2-16-mu-M. Linear calibration graphs passing through the origin were obtained with 25 amines. The method was applied to the identification of biogenic amines from Agrobacterium-transformed plant tissue. Reliability and ease of operation make the procedure particularly well suited to automation, permitting the rapid analysis of a large number of samples.

引用

页码：51 / 57

页数：7

共 20 条

[1] BUSHEY DF, 1987, ANAL BIOCHEM, V167, P36
[2] QUALITATIVE AND QUANTITATIVE MASS-SPECTROMETRY OF SOME NONCATECHOLIC BIOGENIC-AMINES AND RELATED COMPOUNDS AS THEIR DANSYL DERIVATIVES
DURDEN, DA
DAVIS, BA
BOULTON, AA
[J]. BIOMEDICAL MASS SPECTROMETRY, 1974, 1 (02): : 83 - 95
[3] FAGER RS, 1973, ANAL BIOCHEM, V53, P590
[4] ANALYSIS OF POLYAMINES IN HIGHER-PLANTS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
FLORES, HE
GALSTON, AW
[J]. PLANT PHYSIOLOGY, 1982, 69 (03) : 701 - 706
[5] HAYMAN AR, 1985, J CHROMATOGR, V325, P462, DOI 10.1016/S0021-9673(00)96058-8
[6] HYDROXYNORCYTISINE, A QUINOLIZIDONE ALKALOID FROM LABURNUM-ANAGYROIDES
HAYMAN, AR
GRAY, DO
[J]. PHYTOCHEMISTRY, 1989, 28 (02) : 673 - 675
[7] FLUORIGENIC REAGENTS FOR PRIMARY AND SECONDARY-AMINES AND THIOLS IN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY - A REVIEW
IMAI, K
TOYOOKA, T
MIYANO, H
[J]. ANALYST, 1984, 109 (11) : 1365 - 1373
[8] DETECTION OF FLUORESCAMINE-LABELED AMINO-ACIDS, PEPTIDES, AND OTHER PRIMARY AMINES ON THIN-LAYER CHROMATOGRAMS
IMAI, K
BOHLEN, P
STEIN, S
UDENFRIEND, S
[J]. ARCHIVES OF BIOCHEMISTRY AND BIOPHYSICS, 1974, 161 (01) : 161 - 163
[9] DETERMINATION OF DOPAMINE, NOREPINEPHRINE, AND RELATED TRACE AMINES BY PRECHROMATOGRAPHIC DERIVATIZATION WITH NAPHTHALENE-2,3-DICARBOXALDEHYDE
KAWASAKI, T
HIGUCHI, T
IMAI, K
WONG, OS
[J]. ANALYTICAL BIOCHEMISTRY, 1989, 180 (02) : 279 - 285
[10] CHROMOPHORIC LABELING OF AMINO-ACIDS WITH 4-DIMETHYLAMINOAZOBENZENE-4'-SULFONYL CHLORIDE
LIN, JK
CHANG, JY
[J]. ANALYTICAL CHEMISTRY, 1975, 47 (09) : 1634 - 1638

← 1 2 →