LIQUID-CHROMATOGRAPHIC AND MASS-SPECTRAL ANALYSIS OF N,N-DISUBSTITUTED 3,4-METHYLENEDIOXYAMPHETAMINES

被引：6

作者：

CLARK, CR ^{[1
]}

NOGGLE, FT ^{[1
]}

DERUITER, J ^{[1
]}

机构：

[1] ALABAMA DEPT FORENS SCI, AUBURN, AL 36830 USA

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY | 1990年 / 13卷 / 02期

关键词：

D O I：

10.1080/01483919008049542

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The tertiary amine N,N-disubstituted derivatives of 3,4-methylenedioxyamphetamine (MDA) were prepared and their liquid chromatographic and mass spectral properties compared to other analogues of 3,4-methylenedioxyamphetamine. The N-methyl-N-ethyl, N-methyl-N-i-propyl and N-methy1-N-n-propy1 MDA derivatives were separated in a reversed-phase system consisting of a C18stationary phase and a mobile phase of pH 4 phosphate buffer-acetonitrile (55:45). The mass spectral fragmentation of these amines is similar to that observed for the secondary amine MDA derivatives and can be used for their specific structural identification. Copyright © 1990 by Marcel Dekker, Inc.

引用

页码：263 / 274

页数：12

共 8 条

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