STRUCTURE CRISTALLINE DE CH3MGBR.3C4H8O

被引:66
作者
VALLINO, M
机构
[1] Laboratoire de Chimie de l'École Normale Supérieure (Laboratoire de Mécanismes réactionnels), 24, rue Lhomond, Paris 5ème et Laboratoire de Minéralogie et Cristallographie de la Faculté des Sciences, 9, Quai Saint-Bernard
关键词
D O I
10.1016/S0022-328X(00)80080-7
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
The structure of CH3MgBr·3C4H8O was solved by single crystal X-ray diffraction techniques. The five-coordinate magnesium is at the center of a trigonal bipyramide. Methyl and bromine are disordered and tetrahydrofuran rings distorded. A rigid body least square refinement program is described. © 1969.
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