THERMAL-DECOMPOSITION OF ENERGETIC MATERIALS .37. SMATCH FT-IR (SIMULTANEOUS MASS AND TEMPERATURE-CHANGE FT-IR) SPECTROSCOPY

被引：22

作者：

TIMKEN, MD ^{[1
]}

CHEN, JK ^{[1
]}

BRILL, TB ^{[1
]}

机构：

[1] UNIV DELAWARE,DEPT CHEM,NEWARK,DE 19716

来源：

APPLIED SPECTROSCOPY | 1990年 / 44卷 / 04期

关键词：

D O I：

10.1366/0003702904087514

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

This paper describes a newly developed fast thermolysis technique which incorporates the principles described above. We have labeled the technique SMATCH/FT-IR spectroscopy, signifying Simultaneous MAss and Temperature Change/FT-IR spectroscopy. Sample masses of 1 mg or less can be heated at rates up to 320°C/s under 15 psi (abs) argon to a temperature of about 600°C. The cell and experimental procedures are described and illustrated with data for 13.4% N nitrocellulose.

引用

页码：701 / 706

页数：6

共 10 条

[1] POLYMER PYROLYSIS OVER A WIDE-RANGE OF HEATING RATES [J].