SEPARATION AND PURIFICATION OF ORGANOTIN HALIDES

被引:13
作者
JESSEN, EB
TAUGBOL, K
GREIBROKK, T
机构
[1] Department of Chemistry, University of Oslo, Blindern
来源
JOURNAL OF CHROMATOGRAPHY | 1979年 / 168卷 / 01期
关键词
D O I
10.1016/S0021-9673(00)80702-5
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
High-performance liquid chromatography of tin tetrachloride and methylated derivatives of tin tetrachloride has been examined on silanized silica, pyrocarbon silica and styrene-divinylbenzene polymers of different pore sizes. A satisfactory separation of the methylated tin halides and their purification from tin tetrachloride have been achieved by adsorption chromatography on Styragels. These adsorbents have been shown to be of value also for other organotin compounds, and may also be used in studies of redistribution reactions. © 1979.
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页码:139 / 142
页数:4
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