POLAROGRAPHIC STUDY OF AFLATOXINS B1, B2, G1 AND G2 - APPLICATION OF DIFFERENTIAL-PULSE POLAROGRAPHY TO THE DETERMINATION OF AFLATOXIN-B1 IN VARIOUS FOODSTUFFS

被引:13
作者
SMYTH, MR
LAWELLIN, DW
OSTERYOUNG, JG
机构
[1] Department of Microbiology, Colorado State University, Fort Collins
[2] Department of Biochemistry, Medical and Dental School, North Western University, Chicago, IL
关键词
Aflatoxin determination; Differential-pulse polarography; Food analysis;
D O I
10.1039/an9790400073
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The polarographic behaviour of aflatoxins B1, B2, G1 and G2 has been investigated and found to parallel closely that of coumarin and its derivatives. Differential-pulse polarography has been applied to the determination of aflatoxin B1 in a variety of food products. Good agreement was obtained between the differential-pulse polarographic method and visual comparison of the fluorescence exhibited by the aflatoxin following thin-layer chromatographic separation. Electroactive interferences co-extracted from high lipid-containing foods were removed by separation on a Sephadex LH-20 column.
引用
收藏
页码:73 / 78
页数:6
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