SIMPLE PREPARATION OF A BONDED CATION-EXCHANGE PACKING MATERIAL AND ITS APPLICATION TO THE SEPARATION OF PHENOTHIAZINES BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引：44

作者：

WHEALS, BB

机构：

[1] The Metropolitan Police Forensic Science Laboratory, London, 109 Lambeth Rd

来源：

JOURNAL OF CHROMATOGRAPHY | 1979年 / 177卷 / 02期

关键词：

D O I：

10.1016/S0021-9673(01)96322-8

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A method for introducing sulphonic acid groups on to a microparticulate silica is described. This involves formation of a mercaptopropyl bonded phase followed by oxidation to the corresponding sulphonic acid. The packing material so prepared displays cation-exchange properties and has been used to separate phenothiazines. © 1979.

引用

页码：263 / 270

页数：8

共 7 条

[1] HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF PERPHENAZINE AND AMITRIPTYLINE HYDROCHLORIDE IN 2-COMPONENT TABLET FORMULATIONS
BUTTERFIELD, AG
SEARS, RW
[J]. JOURNAL OF PHARMACEUTICAL SCIENCES, 1977, 66 (08) : 1117 - 1119
[2] COMPARISON OF NEW HIGH-CAPACITY ION-EXCHANGE SILICAS OF SPHEROSIL TYPE AND NORMAL MICROPARTICULATE ION-EXCHANGERS OF POLYSTYRENE DIVINYLBENZENE TYPE IN HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
CAUDE, M
ROSSET, R
[J]. JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1977, 15 (09) : 405 - 412
[3] PREPARATION, PROPERTIES AND SOME APPLICATIONS OF BONDED ION-EXCHANGE PACKINGS BASED ON MICROPARTICULATE SILICA-GEL FOR HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
COX, GB
LOSCOMBE, CR
SLUCUTT, MJ
SUGDEN, K
UPFIELD, JA
[J]. JOURNAL OF CHROMATOGRAPHY, 1976, 117 (02): : 269 - 278
[4] PRACTICAL ASPECTS OF BONDED PHASE CHROMATOGRAPHY
COX, GB
[J]. JOURNAL OF CHROMATOGRAPHIC SCIENCE, 1977, 15 (09) : 385 - 392
[5] SOME ASPECTS OF HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY OF FLUPHENAZINE AND ITS ESTERS
HEYES, WF
SALMON, JR
[J]. JOURNAL OF CHROMATOGRAPHY, 1978, 156 (02): : 309 - 316
[6] PRYDE A, 1979, APPLICATIONS HIGH PE
[7] WHEALS BB, 1977, ANALYST, V102, P1218

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