SYNTHESIS OF POTASSIUM HEXATITANATE FIBERS BY THE HYDROTHERMAL DEHYDRATION METHOD

被引：14

作者：

OOTA, T ^{[1
]}

SAITO, H ^{[1
]}

YAMAI, I ^{[1
]}

机构：

[1] NAGOYA INST TECHNOL,CERAM ENGN RES LAB,TAJIMI,JAPAN

来源：

JOURNAL OF CRYSTAL GROWTH | 1979年 / 46卷 / 03期

关键词：

D O I：

10.1016/0022-0248(79)90081-2

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

K2Ti6O13 fibers were synthesized from the system TiO2 · n H2O-KOH-H2O at 390°C for 20 h to investigate: (1) the application of dehydration to the ordinary hydrothermal reaction, (2) the influence of the molar ratio of K2O/TiO2 and the concentration of the KOH solution and (3) the influence of other types of starting materials on crystallization. The so-called hydrothermal dehydration method appeared to be an advantageous technique by which the fibers of some millimeter length were easily formed. Favorable conditions were found to be: 2 N KOH as concentration of solution; about 20% of fill; Zn metal as a dehydration reagent. © 1979.

引用

页码：331 / 338

页数：8

共 10 条

[1]

BERRY KL, 1958, Patent No. 2841470

[2]

ELWELL D, 1975, CRYSTAL GROWTH, V6, P191

[3]

Gier T., 1958, United States Patent, Patent No. 2833620

[4] FIBROUS POTASSIUM TITANATE - A NEW HIGH TEMPERATURE INSULATING MATERIAL [J].

GULLEDGE, HC .

INDUSTRIAL AND ENGINEERING CHEMISTRY, 1960, 52 (02) :117-118

[5]

HOOK AV, 1961, CRYSTALLIZATION THEO, P282

[6]

LAUDISE RA, 1973, CRYSTAL GROWTH INTR, P181

[7] STUDIES ON THE LOWER OXIDES OF TITANIUM [J].

PEARSON, AD .

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1958, 5 (04) :316-+

[8]

Saito H., 1968, J CERAM ASS JAPAN, V76, P247, DOI 10.2109/jcersj1950.76.876_247

[9]

Scheel H. J., 1972, Journal of Crystal Growth, V13-14, P560, DOI 10.1016/0022-0248(72)90516-7

[10]

TAKI S, 1963, KYOGYO KAGAKU ZASSHI, V66, P417

← 1 →