HETERONUCLEAR X-Y DECOUPLING IN THE MAS-NMR SPECTROSCOPY OF INORGANIC SOLIDS

被引：15

作者：

MAXWELL, R ^{[1
]}

LATHROP, D ^{[1
]}

FRANKE, D ^{[1
]}

ECKERT, H ^{[1
]}

机构：

[1] UNIV CALIF SANTA BARBARA,DEPT CHEM,SANTA BARBARA,CA 93106

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH | 1990年 / 29卷 / 08期

关键词：

D O I：

10.1002/anie.199008821

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

31P‐spin decoupling in 113Cd‐ and 77Se‐NMR spectroscopy leads to considerable signal sharpening, as could be demonstrated, for example, with the semiconductor CdGeP2 and the ionic conductor Ag7PSe6. Sample rotation at the magic angle (MAS) and simultaneous irradiation of the 31P resonance frequence furnished, in the case of CdGeP2, the highly resolved 113Cd‐NMR spectrum pictured on the right. (Figure Presented.) Copyright © 1990 by VCH Verlagsgesellschaft mbH, Germany

引用

页码：882 / 884

页数：3

共 10 条

[1] NUCLEAR-MAGNETIC-DOUBLE-RESONANCE INVESTIGATION OF THE DOPANT MICROSTRUCTURE IN HYDROGENATED AMORPHOUS-SILICON [J].

BOYCE, JB ;

READY, SE .

PHYSICAL REVIEW B, 1988, 38 (16) :11008-11018

[2] CHEMISORPTION AND SURFACES STUDIED BY NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY [J].

Duncan, T. M. ;

Dybowski, Cecil .

SURFACE SCIENCE REPORTS, 1981, 1 (04) :157-250

[3]

Guillon T., 1989, J MAGN RESON, V81, P196

[4] LOCAL-STRUCTURE EVALUATION IN SOLID ORGANO-PHOSPHORUS COMPOUNDS BY DOUBLE CROSS POLARIZATION C-13 NUCLEAR MAGNETIC-RESONANCE SPECTROSCOPY [J].

HAGAMAN, EW .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1988, 110 (16) :5594-5595

[5] SIDEBAND INTENSITIES IN NMR-SPECTRA OF SAMPLES SPINNING AT THE MAGIC ANGLE [J].

HERZFELD, J ;

BERGER, AE .

JOURNAL OF CHEMICAL PHYSICS, 1980, 73 (12) :6021-6030

[6] ARGYRODITES - NEW FAMILY OF TETRAHEDRALLY CLOSE-PACKED STRUCTURES [J].

KUHS, WF ;

NITSCHE, R ;

SCHEUNEMANN, K .

MATERIALS RESEARCH BULLETIN, 1979, 14 (02) :241-248

[7]

MACKOWKA CD, 1982, PHYS REV LETT, V49, P379

[8]

MACKOWKA CD, 1985, PHYS REV B, V31, P5663

[9] NMR IN ROTATING SOLIDS [J].

MARICQ, MM ;

WAUGH, JS .

JOURNAL OF CHEMICAL PHYSICS, 1979, 70 (07) :3300-3316

[10] ROTARY RESONANCE RECOUPLING OF DIPOLAR INTERACTIONS IN SOLID-STATE NUCLEAR MAGNETIC-RESONANCE SPECTROSCOPY [J].

OAS, TG ;

GRIFFIN, RG ;

LEVITT, MH .

JOURNAL OF CHEMICAL PHYSICS, 1988, 89 (02) :692-695

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