SIMULTANEOUS DETERMINATION OF VARIOUS PESTICIDES IN WATER BY SOLID-PHASE EXTRACTION HPLC WITH PHOTODIODE-ARRAY DETECTION

被引:13
作者
DELACOLINA, C [1 ]
BAEZ, ME [1 ]
PENA, A [1 ]
ROMERO, E [1 ]
DIOS, G [1 ]
SANCHEZRASERO, F [1 ]
机构
[1] CSIC,ESTAC EXPTL ZAIDIN,PROF ALBAREDA 1,E-18008 GRANADA,SPAIN
关键词
SOLID-PHASE EXTRACTION; REVERSED-PHASE HPLC; PHOTODIODE ARRAY DETECTION; PESTICIDES; WATER;
D O I
10.1016/0048-9697(94)90097-3
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
A solid-phase extraction/high-performance liquid chromatographic method with photodiode array detection has been developed for the simultaneous determination of carbendazim, thiophanate-methyl, lenacil, methabenzthiazuron, diuron, phenmedipham, captan and diflubenzuron in water at the low ng/ml level. Recoveries (82-102%) and precision (R.S.D. 0.5-2.8%) are quite good and the detection limits achieved are up to 2.5 times lower than the maximum limit permitted by the E.C.
引用
收藏
页码:1 / 6
页数:6
相关论文
共 12 条
[2]  
BEAUCHAMP KW, 1989, J ASSOC OFF ANA CHEM, V72, P845
[3]   DETERMINATION OF NONVOLATILE ORGANIC-COMPOUNDS IN AQUEOUS ENVIRONMENTAL-SAMPLES USING LIQUID CHROMATOGRAPHY/MASS SPECTROMETRY [J].
BELLAR, TA ;
BUDDE, WL .
ANALYTICAL CHEMISTRY, 1988, 60 (19) :2076-2083
[4]   EXTRACTION OF ORGANOPHOSPHORUS PESTICIDES FROM WATER SAMPLES ON BAKERBOND SPE OCTADECYL CARTRIDGES AT THE NG/L LEVEL [J].
BORBURGH, HJ ;
HAMMERS, WE .
TOXICOLOGICAL AND ENVIRONMENTAL CHEMISTRY, 1992, 35 (1-2) :79-86
[5]  
CHAU ASY, 1982, ANAL PESTICIDES WATE, V3, P69
[6]   MULTIRESIDUE METHOD FOR PESTICIDES IN DRINKING-WATER USING A GRAPHITIZED CARBON-BLACK CARTRIDGE EXTRACTION AND LIQUID-CHROMATOGRAPHIC ANALYSIS [J].
DICORCIA, A ;
MARCHETTI, M .
ANALYTICAL CHEMISTRY, 1991, 63 (06) :580-585
[7]   INTERFERENCES IN SOLID-PHASE EXTRACTION USING C-18 BONDED POROUS SILICA CARTRIDGES [J].
JUNK, GA ;
AVERY, MJ ;
RICHARD, JJ .
ANALYTICAL CHEMISTRY, 1988, 60 (13) :1347-1350
[8]   RAPID SCREENING OF A LARGE GROUP OF POLAR PESTICIDES IN RIVER WATER BY ONLINE TRACE ENRICHMENT AND COLUMN LIQUID-CHROMATOGRAPHY [J].
LISKA, I ;
BROUWER, ER ;
OSTHEIMER, AGL ;
LINGEMAN, H ;
BRINKMAN, UAT ;
GEERDINK, RB ;
MULDER, WH .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1992, 47 (04) :267-291
[9]   SOLID-PHASE EXTRACTION OF PESTICIDES FROM WATER SAMPLES [J].
MANES, J ;
PICO, Y ;
MOLTO, JC ;
FONT, G .
HRC-JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY, 1990, 13 (12) :843-845
[10]   DETERMINATION OF TRIAZINES AND ORGANOPHOSPHORUS PESTICIDES IN WATER SAMPLES USING SOLID-PHASE EXTRACTION [J].
MOLTO, JC ;
PICO, Y ;
FONT, G ;
MANES, J .
JOURNAL OF CHROMATOGRAPHY, 1991, 555 (1-2) :137-145