GAS-CHROMATOGRAPHIC DETERMINATION OF PESTICIDE-RESIDUES AFTER CLEANUP BY GEL-PERMEATION CHROMATOGRAPHY AND MINI-SILICA GEL-COLUMN CHROMATOGRAPHY

被引：91

作者：

SPECHT, W ^{[1
]}

PELZ, S ^{[1
]}

GILSBACH, W ^{[1
]}

机构：

[1] LANDESUNTERSUCHUNGSAMT GESUNDHEITSWESEN NORDBAYER,D-91054 ERLANGEN,GERMANY

来源：

FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1995年 / 353卷 / 02期

关键词：

D O I：

10.1007/BF00322956

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A new extraction and partition step was introduced into the well established multi-residue method of Specht and Tillkes (DFG method S 19) replacing dichloromethane by ethyl acetate/cyclohexane (1 + 1). In addition, more simple working conditions were obtained. Results of fortification experiments with organochlorine, organophosphorus and organonitrogen pesticides showed good agreement with those obtained by the formerly published method.

引用

页码：183 / 190

页数：8

共 13 条

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[6] GAS-CHROMATOGRAPHIC DETERMINATION OF PESTICIDE-RESIDUES AFTER CLEANUP BY GEL-PERMEATION CHROMATOGRAPHY AND MINI-SILICA GEL-COLUMN CHROMATOGRAPHY .3. COMMUNICATION - CLEANUP OF FOODS AND FEEDS OF VEGETABLE AND ANIMAL ORIGIN FOR MULTIRESIDUE ANALYSIS OF FAT-SOLUBLE AND WATERSOLUBLE PESTICIDES
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