SYNTHESIS OF MILTIRONE BY AN ULTRASOUND-PROMOTED CYCLOADDITION

被引：32

作者：

LEE, JN ^{[1
]}

MEI, HS ^{[1
]}

SNYDER, JK ^{[1
]}

机构：

[1] BOSTON UNIV,DEPT CHEM,590 COMMONWEALTH AVE,BOSTON,MA 02215

来源：

JOURNAL OF ORGANIC CHEMISTRY | 1990年 / 55卷 / 17期

关键词：

D O I：

10.1021/jo00304a010

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The ultrasound-promoted cycloaddition of 3-isopropyl-o-benzoquinone, generated by the in situ silver oxide oxidation of the corresponding catechol, with 6,6-dimethyl-l-vinylcyclohexene has led to the synthesis of miltirone. © 1990, American Chemical Society. All rights reserved.

引用

页码：5013 / 5016

页数：4

共 37 条

[1] NATURALLY OCCURRING QUINONES .11. TANSHINONES
BAILLIE, AC
THOMSON, RH
[J]. JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1968, (01): : 48 - &
[2] DITERPENCHINONES FROM LABIATAE-ROOTS
BRIESKORN, CH
BUCHBERGER, L
[J]. PLANTA MEDICA, 1973, 24 (02) : 190 - 195
[3] CHANG HM, 1986, PHARM APPLICATIONS C, V1, P255
[4] CHIEN MK, 1978, ACTA CHIM SINICA, V36, P199
[5] DROBOVII S, 1977, KHIM PRIR SOEDIN+, P414
[6] SALVIOLONE, A CYTO-TOXIC BISNORDITERPENE WITH A BENZOTROPOLONE CHROMOPHORE FROM A CHINESE DRUG DAN-SHEN (SALVIA-MILTIORRHIZA)
GINDA, H
KUSUMI, T
ISHITSUKA, MO
KAKISAWA, H
WEIJIE, Z
JUR, C
TIAN, GY
[J]. TETRAHEDRON LETTERS, 1988, 29 (36) : 4603 - 4606
[7] ASYMMETRIC SYNTHESES OF SALVIA-MILTIORRHIZA ABIETANOID ORTHO-QUINONES - METHYL TANSHINONATE, TANSHINONE-IIB, TANSHINDIOL-B, AND 3-HYDROXYTANSHINONE
HAIZA, M
LEE, J
SNYDER, JK
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1990, 55 (17) : 5008 - 5013
[8] STRUCTURE OF SALVIOL - NEW PHENOLIC DITERPENE
HAYASHI, T
HANDA, T
OHASHI, M
KAKISAWA, H
HSU, HY
CHEN, YP
[J]. JOURNAL OF THE CHEMICAL SOCIETY D-CHEMICAL COMMUNICATIONS, 1971, (11): : 541 - &
[9] Hayashi T., 1970, J CHEM SOC CHEM COMM, V5, p299a
[10] HONDA G, 1988, CHEM PHARM BULL, V36, P408

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