DETECTION AND IDENTIFICATION OF ANABOLIC-STEROIDS IN BOVINE URINE BY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY

被引：39

作者：

LEBIZEC, B

MONTRADE, MP

MONTEAU, F

ANDRE, F

机构：

[1] ENVN (Ministère de l'Agriculture), Laboratoire des Dosages Hormonaux, 44087 Nantes Cedex 03

来源：

ANALYTICA CHIMICA ACTA | 1993年 / 275卷 / 1-2期

关键词：

GAS CHROMATOGRAPHY MASS SPECTROMETRY; ANABOLIC STEROIDS; BOVINE URINE; HORMONES; URINE;

D O I：

10.1016/0003-2670(93)80283-Q

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Within the scope of the national plan for hormone control in France, a study was made to develop a system for the control of the illegal use of anabolic steroids for fattening purposes in animal production. A screening procedure for these residues in bovine urine was developed, based on C18 solid-phase extraction, silica gel purification and gas chromatographic-mass spectrometric analysis with selected ion monitoring. All the method parameters are discussed, especially the enzymatic and chemical hydrolysis steps and the choice of derivatives.

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页码：123 / 133

页数：11

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