MULTIRESIDUE PROCEDURES FOR THE DETERMINATION OF PESTICIDES IN FOOD USING CAPILLARY GAS-CHROMATOGRAPHIC, FLAME PHOTOMETRIC, AND MASS-SPECTROMETRIC TECHNIQUES

被引:17
作者
MIYAHARA, M
OKADA, Y
TAKEDA, H
AOKI, G
KOBAYASHI, A
SAITO, Y
机构
[1] JAPAN MED FOODS ASSOC,CTR FOOD INSPECT,HIGASHIKURUME,TOKYO 203,JAPAN
[2] YOKOHAMA QUARANTINE OFF,CTR INSPECT IMPORTED FOODS & INFECT DIS,KANAZAWA KU,YOKOHAMA,KANAGAWA 236,JAPAN
[3] NARITA AIRPORT QUARANTINE OFF,NARITA 282,JAPAN
关键词
MULTIRESIDUE PROCEDURES; DETERMINATION OF ORGANOPHOSPHORUS PESTICIDES; CAPILLARY GC; FLAME PHOTOMETRIC DETECTION; MASS SPECTROMETRIC DETECTION;
D O I
10.1021/jf00048a027
中图分类号
S [农业科学];
学科分类号
09 ;
摘要
Organophosphorus pesticides are important for protecting many crops from insects. Multiresidue procedures for 10 organophosphorus pesticides were studied to establish analytical methods using capillary gas chromatography with flame photometric (FPD) and mass spectrometric detector (GCMS). Quantitative gas chromatography with a FPD was examined to determine suitable chromatographic conditions for various GC columns. Gas chromatography with GC-MS was studied to choose proper fragment ions for determination and identification.
引用
收藏
页码:2795 / 2802
页数:8
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