DETERMINATION OF CD, CO, CU, FE AND NI AT PARTS-PER-BILLION LEVEL IN HIGH-PURITY GALLIUM BY GRAPHITE-FURNACE ATOMIC-ABSORPTION SPECTROMETRY (GFAAS)

被引:4
作者
KUMAR, SJ [1 ]
NATARAJAN, S [1 ]
ARUNACHALAM, J [1 ]
GANGADHARAN, S [1 ]
机构
[1] BHABHA ATOM RES CTR,DIV ANALYT CHEM,BOMBAY 400085,INDIA
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1990年 / 338卷 / 07期
关键词
D O I
10.1007/BF00323198
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The determination of Cd, Co, Cu, Fe and Ni in 6N gallium by GFAAS is reported. The analytes are extracted as pyrrolidine dithiocarbamates into methyl-iso-butyl-ketone (MIBK) in the presence of tartrate. The conditions of extraction, quantity of reagents required and the matrix interference aspects are discussed. The method offers one-step matrix removal and preconcentration, leading to low experimental blanks. © 1990 Springer-Verlag.
引用
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页码:836 / 840
页数:5
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