TIME AND TEMPERATURE-DEPENDENCE OF NANOCRYSTALLINE STRUCTURE FORMATION IN A FINEMET-TYPE AMORPHOUS ALLOY

被引:31
作者
VARGA, LK
BAKOS, E
KISDIKOSZO, E
ZSOLDOS, E
KISS, LF
机构
[1] HUNGARIAN ACAD SCI,KFKI,SOLID STATE PHYS RES INST,H-1525 BUDAPEST,HUNGARY
[2] HUNGARIAN ACAD SCI,KFKI,MAT SCI RES INST,POB 49,H-1525 BUDAPEST,HUNGARY
[3] TECH UNIV BUDAPEST,FAC ELECT ENGN,H-1111 BUDAPEST,HUNGARY
关键词
Composition effects - Crystal structure - Deterioration - Grain size and shape - Iron alloys - Magnetic field effects - Magnetic properties - Segregation (metallography) - Thermal effects - X ray analysis;
D O I
10.1016/0304-8853(94)90546-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The magnetic softness and nanocrystalline structure formation of Fe73.5Cu1Nb3Si13.5B9 Finemet alloy as a function of annealing temperature (500-600-degrees-C) and annealing time (5 s-3 h) were investigated by means of magnetic measurements, DSC and X-ray diffractometry. Annealed at 550-degrees-C the grain size, the solute silicon content of alpha-Fe grains and the improvement in magnetic softness saturates as a function of time. The deterioration of the magnetic softness after annealing at 575-degrees-C is attributed to the Fe3Si compound which segregates from the alpha-Fe solid solution, giving a third intermediate peak on the well-known double-peaked DSC diagram. The crystallization products appearing after annealing at 600-degrees-C destroy the intergranular magnetic coupling and give rise to a magnetic hardening.
引用
收藏
页码:280 / 282
页数:3
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