SYNTHESIS AND STRUCTURE OF 1,3-BIS[TRIS(TRIMETHYLSILYL)METHYL]-2,4,5-TRISELENA-1,3-DIGERMABICYCLO[1.1.1]PENTANE

被引：19

作者：

ANDO, W

WATANABE, S

CHOI, NM

机构：

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1995年 / 16期

关键词：

D O I：

10.1039/c39950001683

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

1,3-Bis[tris(trimethylsilyl)methyl]-2,4,5-triselena-1,3-digermabicyclo[1.1.1]pentane 4, obtained by photodeselenation of the corresponding 2,4,5,6-tetraselena-1,3-digermabicyclo[2.1.1]hexane, shows a short Ge ... Ge distance of 2.672 Angstrom; an Se ... Se interaction in 4 is observed by Se-77 NMR, X-ray analysis and electronic spectroscopy.

引用

页码：1683 / 1684

页数：2