A SINGLE-BEAM APPROACH TO THE ABSORPTION-SPECTROSCOPY OF MICROCRYSTALS

被引：59

作者：

KRAUSZ, E

机构：

[1] Research School of Chemistry, The Australian National University, Canberra

来源：

AUSTRALIAN JOURNAL OF CHEMISTRY | 1993年 / 46卷 / 07期

关键词：

D O I：

10.1071/CH9931041

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A single-beam microcrystal absorption spectrometer system is described that operates in the range 300-2600 nm, on crystals smaller than 50 mum, in the temperature range 5-300 K, with resolution better than 1 cm-1. The computer control of data acquisition and baseline storage with interpolation generates data of exceptional quality, and simplifies operation. The salient features of the apparatus are discussed, and the optimal sample absorption is calculated. Examples of optical spectra with relevance to some current interests in inorganic chemistry are provided.

引用

页码：1041 / 1054

页数：14

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