A SOLID-PHASE SPECTROPHOTOMETRIC METHOD FOR THE DETERMINATION OF SULFATHIAZOLE

被引：4

作者：

CAPITANVALLVEY, LF ^{[1
]}

DEORBE, I ^{[1
]}

VALENCIA, MC ^{[1
]}

BERZASNEVADO, JJ ^{[1
]}

机构：

[1] UNIV CASTILLA LA MANCHA,DEPT ANALYT CHEM & FOOD TECHNOL,E-13071 CIUDAD REAL,SPAIN

来源：

TALANTA | 1994年 / 41卷 / 08期

关键词：

D O I：

10.1016/0039-9140(94)E0035-P

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A spectrophotometric method for the determination of sulphathiazole (ST) has been developed, based on solid-phase spectrophotometry. The influence of experimental variables on fixation on Sephadex SP C-25 is discussed. The applicable concentration range is 0.10-10.00 mg/l., with a relative standard deviation of 0.62% and a detection limit of 0.02 mg/l. The accuracy and precision of the method are reported. The proposed method has been satisfactorily applied to the determination of sulphathiazole in pharmaceuticals.

引用

页码：1327 / 1333

页数：7

共 30 条

[1] MONITORING OF VETERINARY DRUG RESIDUES BY A COMBINATION OF CONTINUOUS-FLOW TECHNIQUES AND COLUMN-SWITCHING HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY .1. SULFONAMIDES IN EGG, MEAT AND MILK USING POST-COLUMN DERIVATIZATION WITH DIMETHYLAMINOBENZALDEHYDE [J].

AERTS, MML ;

BEEK, WMJ ;

BRINKMAN, UAT .

JOURNAL OF CHROMATOGRAPHY, 1988, 435 (01) :97-112

[2]

[Anonymous], 1980, ANAL CHEM, V52, P2242

[3]

[Anonymous], 1976, PURE APPL CHEM, V45, P105

[4]

Berzas Nevado J J, 1991, J Pharm Biomed Anal, V9, P117

[5]

Bratton AC, 1939, J BIOL CHEM, V128, P537

[6]

BYE A, 1974, CLIN CHEM, V20, P288

[7] DETERMINATION OF BERYLLIUM IN WATER BY ION-EXCHANGE SPECTROFLUORIMETRY [J].

CAPITAN, F ;

MANZANO, E ;

NAVALON, A ;

VILCHEZ, JL ;

CAPITANVALLVEY, LF .

ANALYST, 1989, 114 (08) :969-973

[8]

CAPITAN F, 1991, ANALUSIS, V19, P177

[9] DETERMINATION OF TITANIUM IN SEAWATER BY ION-EXCHANGE SPECTROPHOTOMETRY [J].

CAPITANVALLVEY, LF ;

VALENCIA, MC ;

DEORBE, I .

MICROCHEMICAL JOURNAL, 1989, 40 (02) :166-174

[10]

DEORBE I, 1991, THESIS U GRANADA

← 1 2 3 →