COMBINED SMALL-ANGLE X-RAY-SCATTERING (SAXS) AND FOURIER-TRANSFORM INFRARED (FT-IR) SPECTROSCOPY IN A TIME-RESOLVED MODE USING SYNCHROTRON-RADIATION

被引:6
作者
BOGG, D
DERBYSHIRE, GE
BRAS, W
COOKE, J
ELWELL, MJA
NAYLOR, S
RYAN, AJ
机构
[1] DRAL,DARESBURY LAB,WARRINGTON WA4 4AD,CHESHIRE,ENGLAND
[2] NETHERLANDS ORG SCI RES,THE HAGUE,NETHERLANDS
[3] UNIV MANCHESTER,INST SCI & TECHNOL,MANCHESTER M60 1QD,LANCS,ENGLAND
关键词
D O I
10.1016/0168-583X(94)00399-8
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
The simultaneous time resolved study of structure development and reaction kinetics during materials processing is an experimental method which has great potential in developing a deeper understanding of the parameters which govern the formation of various material structures and their final properties. A novel combination of synchrotron radiation small angle X-ray scattering and Fourier transform infrared spectroscopy has been developed, at Daresbury Laboratory, to enable these experiments to be conducted. Successful experiments on a series of model segmented block copoly(urethane)s have been performed and have shown that this combination of techniques is feasible, and has the potential to become a very powerful research tool for a wide variety of research fields.
引用
收藏
页码:536 / 538
页数:3
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