DEVELOPMENT OF LARGE-VOLUME REACTION CELLS FOR KINETIC-STUDIES USING ENERGY-DISPERSIVE POWDER DIFFRACTION

被引：50

作者：

CLARK, SM ^{[1
]}

NIELD, A ^{[1
]}

RATHBONE, T ^{[1
]}

FLAHERTY, J ^{[1
]}

TANG, CC ^{[1
]}

EVANS, JSO ^{[1
]}

FRANCIS, RJ ^{[1
]}

OHARE, D ^{[1
]}

机构：

[1] UNIV OXFORD,INORGAN CHEM LAB,OXFORD OX1 3QR,ENGLAND

来源：

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS | 1995年 / 97卷 / 1-4期

关键词：

D O I：

10.1016/0168-583X(94)00415-3

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

Two novel sample chambers for the energy-dispersive powder diffraction study of chemical reactions are presented. One for air sensitive samples and the other for hydrothermal synthesis. The use of these vessels is illustrated with data collected during a study of the intercalation of cobaltocene into SnS2.

引用

页码：98 / 101

页数：4

共 5 条

[1] REAL-TIME IN-SITU X-RAY-DIFFRACTION OF INTERCALATION REACTIONS [J].