SOME REMARKS ON OBTAINING OF VERY PURE P4S9

被引：2

作者：

BRYLEWICZ, Z

RUDNICKI, R

机构：

[1] Department of Basic Chemistry, Warsaw University of Technology, 00-664 Warsaw

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 1994年 / 89卷 / 1-4期

关键词：

TETRAPHOSPHORUS NONASULFIDE SYNTHESIS; EXTRACTION; CRYSTALLIZATION; IR SPECTRA; P-31 NMR SPECTRA;

D O I：

10.1080/10426509408020446

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Pure tetraphosphorus nonasulfide-form P4S9(I)-free of admixtures of other phosphorus sulfides was prepared in two steps. The first one was multistage extraction from the P-S melt containing only P4S9 and P4S7. The second was crystallization of the solid obtained in the first step.

引用

页码：173 / 179

页数：7

共 14 条

[1] P-31 NMR-SPECTRA OF P4S9 AND P4S10 - COMPARISON WITH RELATED COMPOUNDS [J].