SLURRY SAMPLING FOR GRAPHITE-FURNACE ATOMIC-ABSORPTION SPECTROMETRY

被引:91
作者
MILLERIHLI, NJ
机构
[1] US Department of Agriculture, ARS, Nutrient Composition Laboratory, Beltsville, 20705, MD
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1990年 / 337卷 / 03期
关键词
D O I
10.1007/BF00321972
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Slurry preparations are an effective way to introduce solids into the graphite furnace. Ultrasonic agitation keeps samples mixed prior to analysis. Several aspects of the ultrasonic slurry sampling approach are discussed including contamination concerns, analyte partitioning, and the effect of particle size. In addition, sample preparation strategies for slurry preparations of non-powdered materials are reviewed. The suitability of this method for assessing homogeneity is demonstrated. © 1990 Springer-Verlag.
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页码:271 / 274
页数:4
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