QUANTITATION OF AZADIRACHTINS IN INSECTICIDAL FORMULATIONS BY HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY

被引:22
作者
HULL, CJ
DUTTON, WR
SWITZER, BS
机构
[1] Research Division, W. R. Grace and Company, Washington Research Center, Columbia, MD 21044
来源
JOURNAL OF CHROMATOGRAPHY | 1993年 / 633卷 / 1-2期
关键词
D O I
10.1016/0021-9673(93)83167-Q
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A sensitive high-performance liquid chromatographic procedure for the quantitative determination of azadirachting A and estimates of other azadirachtins in insecticidal formulations is described. The procedure utilizes reversed-phase chromatography with detection by UV absorption at 215 nm. The quantitative method described has been found to be accurate to within +/-10% relative between the concentrations of 0.005 and 0.75% (w/w) azadirachtin A in insecticidal formulations of neem kernel extract. The lower limit of detection is 0.001% (w/w).
引用
收藏
页码:300 / 304
页数:5
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