SEPARATION OF STRUCTURAL ISOMERS OF TETRA-TERT-BUTYLPHTHALOCYANINATONICKEL(II)

被引:72
作者
HANACK, M
MENG, DY
BECK, A
SOMMERAUER, M
SUBRAMANIAN, LR
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D O I
10.1039/c39930000058
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Tetra-tert-butylphthalocyaninatonickel is synthesized from phthalic anhydride as well as from phthalodinitrile and nickel chloride, whereby a mixture of four different structural isomers are obtained; two of these isomers, with C2v- and C(s)-symmetry are isolated for the first time by HPLC and medium pressure liquid chromatography (MPLC) and characterized.
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页码:58 / 60
页数:3
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