INVESTIGATION OF THE STRUCTURE OF TRIMETHYLSILYLATED SECONDARY AMIDES BY C-13 NMR-SPECTROSCOPY

被引：13

作者：

MATLIN, SA ^{[1
]}

SAMMES, PG ^{[1
]}

UPTON, RM ^{[1
]}

机构：

[1] CITY UNIV LONDON,DEPT CHEM,LONDON EC1V 4PB,ENGLAND

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1 | 1979年 / 10期

关键词：

D O I：

10.1039/p19790002478

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

13C N.m.r. spectroscopy has been shown to be a further valuable tool for investigating the position of silylation in trimethylsilylated secondary amides. Whereas most lactams are N-silylated and 2-hydroxypyridines O-silylated, acetanilides exist as a mixture of isomers.

引用

页码：2478 / 2480

页数：3

共 11 条

[1]

BIRKOFER L, 1968, NEWER METHODS PREP, V5, P211

[2] NMR SPECTRAL STUDIES OF SOME QUINOLONE DERIVATIVES .5. FURTHER-STUDIES OF C-13 MAGNETIC-RESONANCE SPECTRA OF 2-QUINOLONE AND 4-QUINOLONE DERIVATIVE [J].