GAS CHROMATOGRAPHY OF TRIMETHYLSILYL DERIVATIVES OF IODOTYROSINES AND IODOTHYRONINES

被引：29

作者：

ALEXANDER, NM

SCHEIG, R

机构：

[1] Department of Biochemistry, Yale University School of Medicine, New Haven

[2] Department of Medicine, Yale University School of Medicine, New Haven

来源：

ANALYTICAL BIOCHEMISTRY | 1968年 / 22卷 / 02期

关键词：

D O I：

10.1016/0003-2697(68)90306-0

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Gas chromatographic analysis of the trimethylsilyl derivatives of the iodotyrosines, iodothyronines, tyrosine, and thyronine is described. The silylated derivatives can be synthesized within 5 min at 50° using N,O-bis (trimethylsilyl) acetamide and are readily resolved within 30 min by temperature-programmed gas chromatography. Possible biological applications of this separation technique are discussed. © 1968.

引用

页码：187 / +

页数：1

共 16 条

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