DETERMINATION OF SULPHUR IN FLUOROCARBON POLYMERS BY NEUTRON ACTIVATION

被引:7
作者
HESLOP, RB
TAY, SK
机构
[1] Chemistry Department, The University of Manchester Institute of Science and Technology
关键词
D O I
10.1016/S0003-2670(01)95666-1
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Sulphur can be determined in fluorocarbon polymers and other fluorine compounds by neutron irradiation to convert sulphur-32 to phosphorus-32 by the (n,p) reaction. The phosphorus produced is determined by a substoichiometric extraction of vanadomolybdophosphoric acid, followed by measurement of β-emission. The method is satisfactory for sub-milligram quantities of sulphur irradiated for only 8 h. © 1969.
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页码:183 / &
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