SYNTHESIS AND STRUCTURE OF BENZIODAZOLES

被引：33

作者：

BALTHAZOR, TM

GODAR, DE

STULTS, BR

机构：

[1] Monsanto Agricultural Products Company, Research Department, St. Louis

来源：

JOURNAL OF ORGANIC CHEMISTRY | 1979年 / 44卷 / 09期

关键词：

D O I：

10.1021/jo01323a018

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

N-Alkylbenziodazoles 5a and 5b were prepared by dehydrochlorination of amides 3a and 3b. An X-ray structure determination showed 5b to be a tricoordinate iodinane and not jV-chloroamide 6b. The chemical shift of the carbon a to iodine was found to be sensitive to the oxidation state of iodine. Preparation of a six-membered iodinane heterocycle, 12, was unsuccessful. © 1979, American Chemical Society. All rights reserved.

引用

页码：1447 / 1449

页数：3

共 14 条

[1] SYNTHESIS AND MOLECULAR-STRUCTURE OF 1,3-DIHYDRO-1-HYDROXY-3-METHYL-1,2,3-BENZIODOXAPHOSPHOLE 3-OXIDE
BALTHAZOR, TM
MILES, JA
STULTS, BR
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1978, 43 (23) : 4538 - 4540
[2] ORGANIC POLYVALENT IODINE COMPOUNDS
BANKS, DF
[J]. CHEMICAL REVIEWS, 1966, 66 (03) : 243 - &
[3] SULFURANCES - THEORETICAL ASPECTS OF BONDING, SUBSTITUENT SITE PREFERENCES, AND GEOMETRICAL DISTORTIONS
CHEN, MML
HOFFMANN, R
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1976, 98 (07) : 1647 - 1653
[4] CONFORMATION OF ACYLOXY GROUPS IN I,I-DIACYLOXYIODOBENZENES - DIPOLE-MOMENT STUDY
EXNER, O
PLESNICA.B
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1974, 39 (18) : 2812 - 2814
[5] SOLID-STATE COORDINATION BONDING TO POLYVALENT IODINE - STRUCTURE OF 1-ACETOXY-1,2-BENZIODOXOLIN-3-ONE
GOUGOUTAS, JZ
CLARDY, JC
[J]. JOURNAL OF SOLID STATE CHEMISTRY, 1972, 4 (02) : 226 - +
[6] SYNTHESIS OF BENZIODATHIAZOLES
JAFFE, H
LEFFLER, JE
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1975, 40 (06) : 797 - 799
[7] PARTICIPATION BY ORTHO-SUBSTITUENTS IN THE DISSOCIATION OF IODOBENZENE DICHLORIDES
KEEFER, RM
ANDREWS, LJ
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1959, 81 (20) : 5329 - 5333
[8] KEEFER RM, 1959, J AM CHEM SOC, V81, P4218
[9] HYPERVALENT ORGANOIODINE - CRYSTAL-STRUCTURE OF PHENYLHYDROXYTOSYLOXYIODINE
KOSER, GF
WETTACH, RH
TROUP, JM
FRENZ, BA
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1976, 41 (22) : 3609 - 3611
[10] ORTHO-IODOSOPHENYLPHOSPHORIC ACID
LEFFLER, JE
JAFFE, H
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1973, 38 (15) : 2719 - 2721

← 1 2 →