PYRIDINETHIONES .3. SYNTHESIS OF DITHIOCINES BY REACTION OF 3-FORMYL-2(1H)-PYRIDINETHIONE WITH AMINES - CRYSTAL-STRUCTURE OF THE RESULTING 5,11-IMINO-5H-11H-DIPYRIDO[2,3-B-2',3'-F][1,5]DITHIOCINE RING-SYSTEM

被引：7

作者：

BECHER, J

DREIER, C

SIMONSEN, O

机构：

[1] Department of Chemistry, Odense University

来源：

TETRAHEDRON | 1979年 / 35卷 / 07期

关键词：

D O I：

10.1016/0040-4020(79)80108-8

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The reaction of 3-formyl-2(1H)-pyridinethione and alkyl or aryl primary amines gives rise to a novel imide bridged ring system. The structure 4 of this dithiocine was assigned by synthesis as well as from the spectroscopic data and the X-ray determination. The dithiocine ring was found to have the folded" configuration. The mass spectral fragmentations of the dithiocines were investigated in detail. © 1979."

引用

页码：869 / 873

页数：5

共 25 条

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