LIQUID-CHROMATOGRAPHY OF VITAMIN-B6 WITH ELECTROCHEMICAL DETECTION USING A CARBON-FIBER ELECTRODE

被引:35
作者
HOU, WY [1 ]
JI, HM [1 ]
WANG, EK [1 ]
机构
[1] CHINESE ACAD SCI,CHANGCHUN INST APPL CHEM,CHANGCHUN 130022,PEOPLES R CHINA
关键词
D O I
10.1016/S0003-2670(00)82784-1
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A flow-through electrochemical detector with a carbon fibre electrode was fabricated. A chromatographic method for the determination of vitamin B6 using this detector is described, and the results are compared with those obtained by detection with a thin-layer glassy carbon electrode or spectrophotometry. The detection limit of vitamin B6 is 2.5 ng for pyridoxine, 1 ng for pyridoxal and 1 ng for pyridoxamine. The technique was applied to the determination of vitamin B6 in tablets. © 1990.
引用
收藏
页码:207 / 211
页数:5
相关论文
共 13 条
[1]   POTENTIOMETRIC AND VOLTAMMETRIC RESPONSES OF CARBON-FIBER ELECTRODES [J].
EDMONDS, TE ;
DEAN, JR ;
LATIF, S .
ANALYTICA CHIMICA ACTA, 1988, 212 (1-2) :23-30
[2]   ELECTROANALYTICAL APPLICATIONS OF CARBON-FIBER ELECTRODES [J].
EDMONDS, TE .
ANALYTICA CHIMICA ACTA, 1985, 175 (SEP) :1-22
[3]   LIQUID-CHROMATOGRAPHIC DETERMINATION OF TETRACYCLINE ANTIBIOTICS AT AN ELECTROCHEMICALLY PRE-TREATED GLASSY-CARBON ELECTRODE [J].
HOU, WY ;
WANG, EK .
ANALYST, 1989, 114 (06) :699-702
[4]  
JI H, UNPUB
[5]  
KRULL IS, 1983, AM LAB, V15, P57
[6]  
MALCOLM RS, 1986, ANAL P, V23, P87
[7]   THE BEHAVIOR OF MICROELECTRODES [J].
PONS, S ;
FLEISCHMANN, M .
ANALYTICAL CHEMISTRY, 1987, 59 (24) :A1391-A1399
[8]  
SAMUEL JL, 1981, ANAL P, V18, P24
[9]  
STULIK K, 1986, ANN CHIM-ROME, V76, P315
[10]   DETERMINATION OF DOPA, DOPAMINE, DOPAC, EPINEPHRINE, NOREPINEPHRINE, ALPHA-MONOFLUOROMETHYLDOPA AND ALPHA-DIFLUOROMETHYLDOPA IN VARIOUS TISSUES OF MICE AND RATS USING REVERSED-PHASE ION-PAIR LIQUID-CHROMATOGRAPHY WITH ELECTROCHEMICAL DETECTION [J].
WAGNER, J ;
PALFREYMAN, M ;
ZRAIKA, M .
JOURNAL OF CHROMATOGRAPHY, 1979, 164 (01) :41-54