PREPARATION OF C-14 ENRICHED AND O-18-ENRICHED ALLYL ALCOHOL (PROPANOL FREE)

被引：6

作者：

KUPCZYKSUBOTKOWSKA, L ^{[1
]}

SHINE, HJ ^{[1
]}

机构：

[1] TEXAS TECH UNIV,DEPT CHEM & BIOCHEM,LUBBOCK,TX 79409

来源：

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS | 1992年 / 31卷 / 05期

关键词：

ALLYL ALCOHOL; ALLYL VINYL ETHER; C-14; O-18;

D O I：

10.1002/jlcr.2580310507

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Preparations of specifically labeled [1-C-14]-, [3-C-14]- and [1-O-18]allyl alcohol are described. The syntheses were achieved, respectively, in 7,. 11 and 9 steps, with overall yields of 33%, 10% and 38%. Commercially available (KCN)-C-14, (CH3COONa)-C-14 and (H2O)-O-18 were used as the starting materials.

引用

页码：381 / 385

页数：5

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