STRUCTURE OF TETRAPHENYLARSONIUM BIS(1,2-DITHIOOXALATO-S,S')PALLADATE(II)

被引：13

作者：

ROMAN, P ^{[1
]}

GUTIERREZZORRILLA, JM ^{[1
]}

LUQUE, A ^{[1
]}

BEITIA, JI ^{[1
]}

GUZMANMIRALLES, C ^{[1
]}

MARTINEZRIPOLL, M ^{[1
]}

机构：

[1] CSIC, UEI CRISTALOG, E-28006 MADRID, SPAIN

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1991年 / 47卷

关键词：

D O I：

10.1107/S0108270190007156

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

[As(C6H5)4]2[Pd(C2O2S2)2], M(r) = 1113.37, triclinic, P1BAR, a = 11.101 (7), b = 13.316 (5), c = 18.485 (8) angstrom, alpha = 110.90 (5), beta = 77.74 (8), gamma = 106.28 (8)degrees, V = 2431 (2) angstrom 3, Z = 2, D(m) = 1.53 (1), D(x) = 1.52 g cm-3, lambda(Mo K-alpha) = 0.71069 angstrom, mu = 19.317 cm-1, T = 296 K, F(000) = 1120, R = 0.041, wR = 0.045 for 5034 observed reflections with I > 3-sigma(I). The asymmetric unit of the title compound contains one discrete complex [Pd(C2S2O2)2]2- anion and two [As(C6H5)4]+ cations linked through electrostatic interactions and hydrogen contacts of type C-H...O.

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页码：48 / 51

页数：4

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