TETRAMETHYL TERT-BUTYLCALIX[4]ARENE TETRAKETONE

被引：2

作者：

FERGUSON, G ^{[1
]}

GALLAGHER, JF ^{[1
]}

MCKERVEY, MA ^{[1
]}

机构：

[1] QUEENS UNIV BELFAST,DEPT CHEM,BELFAST BT9 5AG,NORTH IRELAND

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1993年 / 49卷 / 03期

关键词：

Molecules;

D O I：

10.1107/S0108270192010515

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title molecule, 25,26,27,28-tetraacetonyloxy-5,11,-17,23-tetra-tert-butylpentacyclo[19.3. 1.1(3,7).1(9,13).1(15,19)]-octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19,21,23-dodecaene, has twofold crystallographic symmetry and adopts a distorted cone conformation in the solid state. The orientation of the four aromatic rings is such that two of the rings are almost parallel to each other and the other two almost normal to one another. This conformation precludes a solvent molecule being enclathrated within the cavity.

引用

页码：602 / 604

页数：3

共 4 条

[1] SYNTHESIS, X-RAY CRYSTAL-STRUCTURES, AND CATION-BINDING PROPERTIES OF ALKYL CALIXARYL ESTERS AND KETONES, A NEW FAMILY OF MACROCYCLIC MOLECULAR RECEPTORS
ARNAUDNEU, F
COLLINS, EM
DEASY, M
FERGUSON, G
HARRIS, SJ
KAITNER, B
LOUGH, AJ
MCKERVEY, MA
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RUHL, BL
SCHWINGWEILL, MJ
SEWARD, EM
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (23) : 8681 - 8691
[2] NRCVAX - AN INTERACTIVE PROGRAM SYSTEM FOR STRUCTURE-ANALYSIS
GABE, EJ
LEPAGE, Y
CHARLAND, JP
LEE, FL
WHITE, PS
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1989, 22 : 384 - 387
[3] JOHNSON CK, 1976, ORNL5138 REP
[4] SPEK AL, 1991, PLATON MOL GEOMETRY

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