BACKGROUND CORRECTION IN FREQUENCY-MODULATED SIMULTANEOUS ATOMIC-ABSORPTION SPECTROMETRY

被引:6
作者
LEHNERT, R [1 ]
QUICK, L [1 ]
RUMP, T [1 ]
WINTER, F [1 ]
CAMMANN, K [1 ]
机构
[1] UNIV MUNSTER,IST ANALYT CHEM,INST CHEM & BIOSENSORIK V,WILHELM KLEMM STR 8,W-4400 MUNSTER,GERMANY
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1993年 / 346卷 / 04期
关键词
D O I
10.1007/BF00325849
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
For a long time simultaneous multielement determination by AAS has been a subject of intensive research. In this work a simultaneous multielement atomic absorption spectrometry method is described in a special new arrangement, called frequency modulated simultaneous AAS (FremsAAS), using fiberoptics, interference filters and frequency modulation and demodulation by lock-in amplifiers as main devices. Purpose of this work was to equip the FremsAAS with a D2-background correction and to test it with certified reference materials. Mn, Cd, Pb, Cu, Ni, Cr and Zn had been determined simultaneously (three at a time) in sewage sludge (BCR/CRM 146), estuarine sediment (BCR/CRM 277) and phosphate rock (BCR/CRM 32) with good feasibility. Frequency modulated simultaneous AAS with background correction (FremsAASUK) represents an interesting alternative to known instruments.
引用
收藏
页码:392 / 395
页数:4
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