BIS(TRIPHENYLPHOSPHINE)IMINIUM HEXAFLUOROPHOSPHATE DICHLOROMETHANE SOLVATE-(1/1)

被引:3
作者
BLAKE, AJ
FREEMAN, G
JOHNSON, BFG
MCDOUGALL, GS
机构
关键词
D O I
10.1107/S010827019400140X
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Bis(triphenylphosphine)iminium hexafluorophosphate [or bis(phosphoranylidene) ammonium hexafluorophosphate] crystallizes from dichloromethane/hexane as a (1/1) solvate, [C36H30NP2][PF6].CH2Cl2, in which the CH2Cl2 molecule is extensively disordered. The cation and anion are essentially ions linked by some short intermolecular contacts.
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页码:1301 / 1303
页数:3
相关论文
共 10 条
  • [1] THE SYNTHESIS OF THE 1ST DECAMETAL NITRIDO CLUSTER - X-RAY STRUCTURE-ANALYSIS AND N-14 NMR-STUDIES OF [(PH3P)2N][RU10N(CO)24]
    BAILEY, PJ
    CONOLE, GC
    JOHNSON, BFG
    LEWIS, J
    MCPARTLIN, M
    MOULE, A
    WILKINSON, DA
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1991, 30 (12): : 1706 - 1707
  • [2] BLAKE AJ, 1994, UNPUB
  • [3] SYNTHESIS AND CRYSTAL AND MOLECULAR-STRUCTURE OF [(PH3P)2N+][S4N-] AND THE ELECTRONIC-STRUCTURE OF THE PLANAR ACYCLIC ANION, S4N-1
    CHIVERS, T
    LAIDLAW, WG
    OAKLEY, RT
    TRSIC, M
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1980, 102 (18) : 5773 - 5781
  • [4] THE MULTIPLY BONDED OCTACHLORODIOSMATE(III) ANION [OS2CL8]2- - THE 1ST EXAMPLE OF A HOMOLEPTIC HALIDE COMPLEX OF THIS TYPE FOR THE PLATINUM METALS
    FANWICK, PE
    KING, MK
    TETRICK, SM
    WALTON, RA
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1985, 107 (17) : 5009 - 5011
  • [5] OPENING OF AN AZA-CLOSO-DODECABORANE TO AN AZA-NIDO-DODECABORATE
    MEYER, F
    MULLER, J
    PAETZOLD, P
    BOESE, R
    [J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH, 1992, 31 (09): : 1227 - 1229
  • [6] PHASE ANNEALING IN SHELX-90 - DIRECT METHODS FOR LARGER STRUCTURES
    SHELDRICK, GM
    [J]. ACTA CRYSTALLOGRAPHICA SECTION A, 1990, 46 : 467 - 473
  • [7] SHELDRICK GM, 1994, UNPUB J APPL CRYST
  • [8] SHELDRICK GM, 1992, SHELXTL USER MANUAL
  • [9] 1988, DIF4 DIFFRACTOMETER
  • [10] 1988, REDU4 DATA REDUCTION