AN EFFICIENT PREPARATION OF POTASSIUM BIS(TRIMETHYLSILYL)AMIDE (KHMDS)

被引：11

作者：

AHMAN, J ^{[1
]}

SOMFAI, P ^{[1
]}

机构：

[1] LUND UNIV,LUND INST TECHNOL,CTR CHEM,S-22100 LUND,SWEDEN

来源：

SYNTHETIC COMMUNICATIONS | 1995年 / 25卷 / 15期

关键词：

D O I：

10.1080/00397919508011786

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A mild and reliable procedure for the preparation of potassium bis(trimethylsilyl)amide (KHMDS) in THF is described.

引用

收藏

页码：2301 / 2303

页数：3

相关论文

共 4 条

[1] AHMAN J, 1994, J AM CHEM SOC, V116, P9781
[2] POTASSIUM HYDRIDE, A HIGHLY ACTIVE NEW HYDRIDE REAGENT - REACTIVITY, APPLICATIONS, AND TECHNIQUES IN ORGANIC AND ORGANOMETALLIC REACTIONS
BROWN, CA
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1974, 39 (26) : 3913 - 3918
[3] TOTAL SYNTHESIS OF THE IONOPHORE ANTIBIOTIC CP-61,405 (ROUTIENNOCIN)
DIEZMARTIN, D
KOTECHA, NR
LEY, SV
MANTEGANI, S
MENENDEZ, JC
ORGAN, HM
WHITE, AD
BANKS, BJ
[J]. TETRAHEDRON, 1992, 48 (37) : 7899 - 7938
[4] CONVENIENT METHOD FOR THE TITRATION OF AMIDE BASE SOLUTIONS
IRELAND, RE
MEISSNER, RS
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1991, 56 (14) : 4566 - 4568