MICRO COPRECIPITATION TECHNIQUE FOR USE IN X-RAY-FLUORESCENCE ANALYSIS

被引:9
作者
KESSLER, JE
VINCENT, SM
RILEY, JE
机构
[1] Analytical Chemistry Research Department, Bell Laboratories, Murray Hill
关键词
D O I
10.1016/0039-9140(79)80148-4
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An apparatus and a procedure are described for the preconcentration of nanogram amounts of trace elements. Co-precipitation and pressure filtration confine the precipitate to a 1.27 mm diameter spot on a filter membrane. Trace elements in the 10-10O ng range are collected reproducibly and detected with high sensitivity by X-ray fluorescence, by use of a milliprobe instrument. Advantages of the technique for quantitative applications are discussed. © 1979.
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页码:21 / 24
页数:4
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