A RAPID GAS-CHROMATOGRAPHY METHOD FOR QUANTITATION OF FREE FATTY-ACIDS, MONOACYLGLYCEROLS, DIACYLGLYCEROLS, AND TRIACYLGLYCEROLS WITHOUT DERIVATIZATION

被引:7
作者
KWON, SJ
LEE, SY
CHO, SW
RHEE, JS
机构
[1] KOREA ADV INST SCI & TECHNOL,DEPT BIOTECHNOL,373-1 KUSONG DONG,TAEJON 305701,SOUTH KOREA
[2] DOOSAN TECH CTR,KYONGGI DO 449840,SOUTH KOREA
关键词
D O I
10.1007/BF00152621
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Quantitative analysis of mixtures of free fatty acids, monoacyl-, diacyl-, and triacylglycerols by a simple and rapid gas chromatography method has been developed. The analysis was carried out on a short capillary column without derivatization. When the triacontane was used as an internal standard, we obtained relative response factors for each lipid class with reproducibility and accuracy. This method could be applied for not only compositional analysis of fats and oils but also monitoring lipase reactions.
引用
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页码:727 / 732
页数:6
相关论文
共 8 条
[1]  
Christie W.W., 1989, GAS CHROMATOGRAPHY L
[2]   DETERMINATION OF MONOCERIDES AND DIGLYCERIDES IN PALM OIL, OLEIN AND STEARIN [J].
GOH, EM ;
TIMMS, RE .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1985, 62 (04) :730-734
[3]  
HIRSH J, 1958, J BIOL CHEM, V233, P312
[4]  
KUKSIS A, 1967, LIPID CHROMATOGRAPHI, V1, P239
[5]   APPLICATION OF GAS-LIQUID PARTITION CHROMATOGRAPHY TO THE QUANTITATIVE ESTIMATION OF MONOGLYCERIDES [J].
MCINNES, AG ;
TATTRIE, NH ;
KATES, M .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1960, 37 (01) :7-11
[6]   QUANTITATIVE ESTIMATION OF ISOMERIC MONOGLYCERIDES BY THIN-LAYER CHROMATOGRAPHY [J].
THOMAS, AE ;
SCHAROUN, JE ;
RALSTON, H .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1965, 42 (09) :789-+
[7]   GAS-LIQUID CHROMATOGRAPHIC ANALYSIS OF MONOGLYCERIDES AS THEIR TRIMETHYLSILYL ETHER DERIVATIVES [J].
WOOD, RD ;
RAJU, PK ;
REISER, R .
JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1965, 42 (03) :161-&
[8]  
YAMANE T, 1986, J JPN OIL CHEM SOC, V35, P45