IMPROVED SYNTHESIS AND CRYSTAL-STRUCTURE OF TETRAKIS(BENZOYLTHIO)-TETRATHIAFULVALENE - A USEFUL PRECURSOR TO FUNCTIONALIZED BIS(ETHYLENEDITHIO)TETRATHIAFULVALENE DERIVATIVES

被引：14

作者：

HANSEN, TK

HAWKINS, I

VARMA, KS

EDGE, S

LARSEN, S

BECHER, J

UNDERHILL, AE

机构：

[1] UNIV WALES,DEPT CHEM,BANGOR LL57 2UW,GWYNEDD,WALES

[2] UNIV COPENHAGEN,DEPT CHEM,DK-2100 COPENHAGEN,DENMARK

来源：

JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2 | 1991年 / 12期

关键词：

D O I：

10.1039/p29910001963

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A simple one-step procedure is reported for the preparation of tetrakis(benzoylthio)tetrathiafulvalene (2) using octacarbonyldicobalt. The crystal structure of 2 is discussed and the preparation of some charge-transfer salts of 2 and their electrical conductivity has been determined. The use of 2 as a synthon for functionalised bis(ethylenedithio)tetrathiafluvalene derivatives is described.

引用

页码：1963 / 1965

页数：3

共 14 条

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